The mixture was refined by sodium sulfide and sodium hydroxide to afford an O,O-diethyl thiophosphoryl chloride at a purity of 99%.
该粗品通过精制工艺的改
,采用硫化钠和氢氧化钠的混合
处理,得到纯度≥99%的O,O-二
基硫代磷酰氯。
The mixture was refined by sodium sulfide and sodium hydroxide to afford an O,O-diethyl thiophosphoryl chloride at a purity of 99%.
该粗品通过精制工艺的改,采用硫化钠和氢氧化钠的混合处理,得到纯度≥99%的O,O-二基硫代磷酰氯。
Ethyl cellulose was synthesized successfully in one step based on reaction of cellulose with excess chloroethane and sodium hydroxide in toluene as diluent.
采用
与过量的氯烷及氢氧化钠反应,以甲苯为稀释剂,用一步法成功地合成了基。
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