Methyl thioacetate was prepared by using acetyl chloride and methyl mercaptan as starting raw material in this paper.The yield of product is 69.3%.Itcan be used in seasoning flavor.

对可用于各种调味食用料硫代乙酸甲酯合成进行了步研究，产率达到693％，对所合成产品做了谱分析和质子核磁共振分析，确定了其化学结构。