Application of samarium diiodide in mediating intramolecular cyclization reactions was reviewed.
综述了二碘钐在分子内
反应中的应用。
Application of samarium diiodide in mediating intramolecular cyclization reactions was reviewed.
综述了二碘钐在分子内
反应中的应用。
Levocetirizine Dihydrochloride was prepared from benzoyl chloride by acidylation,hydrogenation,cyclization with an overall yield of 8.05%.
以苯甲氯
原料,经
,还原,
合等反应合成左旋西替利嗪盐酸盐,反应总收率
8.05%。
Method The target compound was synthesized from clarithromycin via hydrolyzation,acetylation,cyclic carbonatation,oxidation,decarbonatation,acylation,cyclic carbamatation and cyclization.
方法以克拉霉始原料,经水解、乙
、
酸酯
、氧
、脱
酸酯
、
、
氨基甲酸酯
和
合等反应合成目标
合物。
N butyl 2 ethoxy thioacridone was prepared from o chloro benzoic acid and p phenetidine by means of Ullman reaction,cyclization,N alkylation and sulfurization.
以邻氯苯甲酸和对乙氧基苯胺原料,经过胺的苯基
、二芳胺的
、N-烷基
、硫代
反应合成了N-丁基-2-乙氧基硫代吖啶酮。
This paper reports the improvement on the synthesis of 5 methylisoxazol 3 formamide by Claisen condensation of diethyl oxalacetate followed by cyclization and ammonolysis.
讨论了以草酸二乙酯原料,经过克莱森缩合、
合、氨解反应合成5甲基异唑3甲
胺工艺的改进。
In this paper, the synthesis of 2 - chloranthraquinone and 2 - aminoanthraquinone was studied.It was prepared from phthalic anhydride by acetyiation, hydrolysis and cyclization.
以苯酐和取代苯原料,经过乙
、水解及
合反应,合成了2-氯蒽醌和2-氨基蒽醌,并对影响收率的工艺条件进行了研究。
Aqueous titanium trichloride promoted intermolecular reductive cyclization of 1,2 -diketone and o-nitroaniline in basic media provides a convenient method for the synthesis of quinoxaline derivatives.
本文研究了三氯钛水溶液作用下,邻硝基苯胺与1,2-二酮在碱性介质中分子间的成
反应,提供了一个方便地合成取代喹喔啉类
合物的方法。
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